By A. Andreatti, W. Stoll
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Extra info for Analytic and Algebraic Dependence of Meromorphic Fns
K. SUDIANA, G . G. 1 1 H-NMR Spectrum The 270 MHz 'H-NMR spectrum of citric acid was obtained in deuterated methanol using a JEOL JNM LA-270 spectrometer, and is shown in Figure 9. All chemical shifts arc: reported as 6 values (ppm) relative to tetramethylsilane (TMS) and re: idual CD30D as internal standards. The assignments for the observed bands are found in Table 13, together with multiplicities and coupling constants. 2 13 C-NMR Spectrum The broadband decoupled I3C-NMR spectrum of citric acid is shown in Figure 10.
T. K. SUDIANA, G. G. 83 C(2), (34) Figure 1 1. CITRIC ACID Chemical ionization mass spectrum of citric acid. 43 44 Electron impact mass spectrum of citric acid. H. POERWONO, K. HIGASHIYAMA, H. T. K. SUDIANA, G. G. BRITTAIN Figure 12. 5) [M + 1 (H) - 90 (2 x C02H)I' CI (Isobutane) 46 H. POERWONO. K. HIGASHIYAMA, H. KUBO. T. K. SUDIANA, G. G. 1 Identification According to the United States Pharmacopoeia 24 , citric acid is identified by using a solution of the analyte responds to the test for Citrate (pyridine - acetic anhydride test) <191>.
05 mg of the monohydrate. 1 Methods of the United States and Indonesian Pharmacopoeias Both the Indonesian Pharmacopcseia 1995 [ 101 and the Unites States Pharmacopoeia 24  use the scimeprocedure. About 3 g of citric acid (accurately weighed) is dissolvec in 40 mL of water, phenolphthalein TS is added, and the resulting solution is titrated with 1 N sodium hydroxide to a pink end-point. 5 g of citric acid sample is accurately weighed and dissolved in 40 mL sf freshly boiled and cooled water.